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The Effects of Sintering Additives on the Sintering of 3Y-TZP Ceramic
Journal
IOP Conference Series: Materials Science and Engineering
ISSN
1757-8981
Date Issued
2021-03-01
Author(s)
S Theenagaran
C H Ting
K L Chin
W H Yeo
C K Ng
S Ramesh
W D Teng
DOI
https://iopscience.iop.org/article/10.1088/1757-899X/1117/1/012010
Abstract
<jats:title>Abstract</jats:title>
<jats:p>The influence of 0.5 wt.% of manganese oxide (MnO2) addition as dopant into 3 mol% yttria stabilized tetragonal zirconia polycrystals (3Y-TZP) were studied in comparison to undoped 3Y-TZP using different sintering profiles. Samples were sintered at 1200°C, 1300°C and 1400°C with holding time of 1 min, 12 min, 2 hours and 20 hours all for single step sintering. The optimal sintering profiles are A4 and C2 where 3Y-TZP doped with 0.5% wt. MnO2 sintered at 1400°C for 12 minutes and 1200 °C for 20 hours respectively. At these sintering parameters, the MnO2 doped 3Y-TZP sample exhibited relative density of ~97%, Vicker’s Hardness value of ~13 GPa, Fracture toughness value of ~4 MPam1/2 and Young’s modulus of ~210 GPa.</jats:p>
<jats:p>The influence of 0.5 wt.% of manganese oxide (MnO2) addition as dopant into 3 mol% yttria stabilized tetragonal zirconia polycrystals (3Y-TZP) were studied in comparison to undoped 3Y-TZP using different sintering profiles. Samples were sintered at 1200°C, 1300°C and 1400°C with holding time of 1 min, 12 min, 2 hours and 20 hours all for single step sintering. The optimal sintering profiles are A4 and C2 where 3Y-TZP doped with 0.5% wt. MnO2 sintered at 1400°C for 12 minutes and 1200 °C for 20 hours respectively. At these sintering parameters, the MnO2 doped 3Y-TZP sample exhibited relative density of ~97%, Vicker’s Hardness value of ~13 GPa, Fracture toughness value of ~4 MPam1/2 and Young’s modulus of ~210 GPa.</jats:p>
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